Mostrando 10 resultados de: 12
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Journal of Chromatography A(4)
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Journal of Pharmaceutical and Biomedical Analysis(1)
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scopus(12)
Comparative enantioseparation of ketoprofen with trimethylated α-, β-, and γ-cyclodextrins in capillary electrophoresis and study of related selector-selectand interactions using nuclear magnetic resonance spectroscopy
ArticleAbstract: The enantiomers of ketoprofen were separated by capillary electrophoresis using the (2,3,6-tri-O-metPalabras claves:1D ROESY, capillary electrophoresis, cyclodextrins, enantiomer affinity pattern, ketoprofen, nuclear magnetic resonance spectroscopy, Separation mechanismAutores:Antonio Salgado, Chankvetadze B., Samakashvili S., Scriba G.K.E.Fuentes:scopusComplexation of daclatasvir by single isomer methylated β-cyclodextrins studied by capillary electrophoresis, NMR spectroscopy and mass spectrometry
ArticleAbstract: In capillary electrophoresis an enantioseparation of daclatasvir (DCV) was observed in case of heptaPalabras claves:capillary electrophoresis, Complex stoichiometry, Complex structure, Cyclodextrin-analyte complexation, Mass spectrometry, nuclear magnetic resonance spectroscopyAutores:Antonio Salgado, Benkovics G., Chankvetadze B., Krait S., Malanga M., Naumann L., Neusüß C., Peluso P., Scriba G.K.E., Sohajda T.Fuentes:scopusCapillary electrophoretic and nuclear magnetic resonance studies on the opposite affinity pattern of propranolol enantiomers towards various cyclodextrins
ArticleAbstract: In the present study the migration order of the propranolol enantiomers with various native CDs andPalabras claves:capillary electrophoresis, cyclodextrins, enantiomer migration order, NMR spectroscopy, Propranolol, Separation mechanismsAutores:Antonio Salgado, Chankvetadze B., Crommen J., Fillet M., Lomsadze K., Rousseau A., Servais A.Fuentes:scopusApplications of nuclear magnetic resonance spectroscopy for the understanding of enantiomer separation mechanisms in capillary electrophoresis
ReviewAbstract: This review deals with the applications of nuclear magnetic resonance (NMR) spectroscopy to understaPalabras claves:capillary electrophoresis, Chiral recognition mechanisms, Enantioseparations, NMR spectroscopyAutores:Antonio Salgado, Chankvetadze B.Fuentes:scopusEnantiomeric separation of ivabradine by cyclodextrin-electrokinetic chromatography. Effect of amino acid chiral ionic liquids
ArticleAbstract: A chiral methodology was developed for the first time to ensure the quality control of ivabradine, aPalabras claves:capillary electrophoresis, Chiral ionic liquids, chromatography, cyclodextrins, Electrokinetic, Enantioseparation, IvabradineAutores:Antonio Salgado, Casado N., Castro-Puyana M., García M.Á., Marina M.L.Fuentes:scopusEnantiomeric separation of the antiuremic drug colchicine by electrokinetic chromatography. Method development and quantitative analysis
ArticleAbstract: Two analytical methodologies were developed by CE enabling the enantiomeric separation of colchicinePalabras claves:capillary electrophoresis, colchicine, enantiomer migration order, Enantioseparation, H NMR, QuantitationAutores:Antonio Salgado, Castro-Puyana M., García M.Á., Marina M.L., Menéndez-López N., Valimaña-Traverso J.Fuentes:scopusNuclear magnetic resonance to study the interactions acting in the enantiomeric separation of homocysteine by capillary electrophoresis with a dual system of γ-cyclodextrin and the chiral ionic liquid EtCholNTf<inf>2</inf>
ArticleAbstract: The enantiomeric separation of 9-fluorenylmethoxycarbonyl chloride (FMOC)-homocysteine (Hcy) by CE wPalabras claves:capillary electrophoresis, Chiral ionic liquids, homocysteine, NMRAutores:Antonio Salgado, Castro-Puyana M., Greño M., Marina M.L.Fuentes:scopusInvestigation on the enantioseparation of duloxetine by capillary electrophoresis, NMR, and mass spectrometry
ArticleAbstract: The enantiomeric separation of the antidepressant drug duloxetine was investigated by CE using 15 nePalabras claves:capillary electrophoresis, cyclodextrins, Duloxetine, enantiomer migration order, Separation mechanismAutores:Antonio Salgado, Crego A.L., Marina M.L., Sánchez-López E.Fuentes:scopusUnusual complexation behavior between daclatasvir and γ-Cyclodextrin. A multiplatform study
ArticleAbstract: During a screening of cyclodextrins (CDs) as chiral selectors for the separation of daclatasvir (DCVPalabras claves:capillary electrophoresis, Complex stoichiometry, Complex structure, Cyclodextrin, Nuclear magnetic resonance, Selector-selectand complexationAutores:Antonio Salgado, Chankvetadze B., Krait S., Naumann L., Neusüß C., Scriba G.K.E., Villani C.Fuentes:scopusSeparation of tetrahydrozoline enantiomers in capillary electrophoresis with cyclodextrin-type chiral selectors and investigation of chiral recognition mechanisms
ArticleAbstract: The recognition power and affinity pattern of various cyclodextrins (CD) towards the enantiomers ofPalabras claves:capillary electrophoresis, Chiral recognition mechanism, cyclodextrins, molecular modeling, nuclear magnetic resonance spectroscopy, TetrahydrozolineAutores:Antonio Salgado, Chankvetadze B., Chankvetadze L., Dallocchio R., Gogolashvili A., Lomsadze K., Peluso P., Takaishvili N.Fuentes:scopus