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Journal of Chromatography A(4)
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Capillary electrophoretic and nuclear magnetic resonance studies on the opposite affinity pattern of propranolol enantiomers towards various cyclodextrins
ArticleAbstract: In the present study the migration order of the propranolol enantiomers with various native CDs andPalabras claves:capillary electrophoresis, cyclodextrins, enantiomer migration order, NMR spectroscopy, Propranolol, Separation mechanismsAutores:Antonio Salgado, Chankvetadze B., Crommen J., Fillet M., Lomsadze K., Rousseau A., Servais A.Fuentes:scopusApplications of nuclear magnetic resonance spectroscopy for the understanding of enantiomer separation mechanisms in capillary electrophoresis
ReviewAbstract: This review deals with the applications of nuclear magnetic resonance (NMR) spectroscopy to understaPalabras claves:capillary electrophoresis, Chiral recognition mechanisms, Enantioseparations, NMR spectroscopyAutores:Antonio Salgado, Chankvetadze B.Fuentes:scopusComparative enantioseparation of ketoprofen with trimethylated α-, β-, and γ-cyclodextrins in capillary electrophoresis and study of related selector-selectand interactions using nuclear magnetic resonance spectroscopy
ArticleAbstract: The enantiomers of ketoprofen were separated by capillary electrophoresis using the (2,3,6-tri-O-metPalabras claves:1D ROESY, capillary electrophoresis, cyclodextrins, enantiomer affinity pattern, ketoprofen, nuclear magnetic resonance spectroscopy, Separation mechanismAutores:Antonio Salgado, Chankvetadze B., Samakashvili S., Scriba G.K.E.Fuentes:scopusComplexation of daclatasvir by single isomer methylated β-cyclodextrins studied by capillary electrophoresis, NMR spectroscopy and mass spectrometry
ArticleAbstract: In capillary electrophoresis an enantioseparation of daclatasvir (DCV) was observed in case of heptaPalabras claves:capillary electrophoresis, Complex stoichiometry, Complex structure, Cyclodextrin-analyte complexation, Mass spectrometry, nuclear magnetic resonance spectroscopyAutores:Antonio Salgado, Benkovics G., Chankvetadze B., Krait S., Malanga M., Naumann L., Neusüß C., Peluso P., Scriba G.K.E., Sohajda T.Fuentes:scopusStructural characterization of methyl-β-cyclodextrins by high-performance liquid chromatography and nuclear magnetic resonance spectroscopy and effect of their isomeric composition on the capillary electrophoresis enantioseparation of daclatasvir
ArticleAbstract: The separation of daclatasvir and its R,R,R,R-enantiomer was studied by capillary electrophoresis usPalabras claves:capillary electrophoresis, Cyclodextrin isomers, Degree of substitution, enantiomer migration order, Enantioseparation, Methyl-β-cyclodextrinAutores:Antonio Salgado, Benkovics G., Chankvetadze B., Krait S., Malanga M., Scriba G.K.E., Sohajda T., Szakály P.S.Fuentes:scopusUnusual complexation behavior between daclatasvir and γ-Cyclodextrin. A multiplatform study
ArticleAbstract: During a screening of cyclodextrins (CDs) as chiral selectors for the separation of daclatasvir (DCVPalabras claves:capillary electrophoresis, Complex stoichiometry, Complex structure, Cyclodextrin, Nuclear magnetic resonance, Selector-selectand complexationAutores:Antonio Salgado, Chankvetadze B., Krait S., Naumann L., Neusüß C., Scriba G.K.E., Villani C.Fuentes:scopusSeparation of tetrahydrozoline enantiomers in capillary electrophoresis with cyclodextrin-type chiral selectors and investigation of chiral recognition mechanisms
ArticleAbstract: The recognition power and affinity pattern of various cyclodextrins (CD) towards the enantiomers ofPalabras claves:capillary electrophoresis, Chiral recognition mechanism, cyclodextrins, molecular modeling, nuclear magnetic resonance spectroscopy, TetrahydrozolineAutores:Antonio Salgado, Chankvetadze B., Chankvetadze L., Dallocchio R., Gogolashvili A., Lomsadze K., Peluso P., Takaishvili N.Fuentes:scopus