A new methodology based on TRU resin to measure U-, Th-isotopes and <sup>210</sup>Po by alpha-particle spectrometry
Abstract:
This report presents a new methodology to isolate and measure 210Po, as well as uranium and thorium isotopes. This new methodology reduces the standard time of operation, the minimum amount of chemical reagents and the quantity of resin used in comparison with other standard and well-established procedures for alpha spectrometry. Thus, the amount of chemicals reagent was lower than the amount used in other standard radiochemical processes: only 6 mL of 1 M HCl was used for the thorium elution, and 2 mL of H2O and 1 mL of Ammonium Oxalate (0.05 M) (3 mL in total) for the uranium elution. Likewise, many samples of various activities and materials (liquids and solids) were used to validate the method.
Año de publicación:
2023
Keywords:
- sequential extraction
- 210 Po
- Alpha spectrometry
- Environmental radioactivity samples
- U- and Th- Isolation
- TRU resin
Fuente:
scopus
Tipo de documento:
Article
Estado:
Acceso restringido
Áreas de conocimiento:
- Química analítica
- Ciencia de materiales
Áreas temáticas:
- Química analítica
- Química inorgánica