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A new strategy for solid-phase depsipeptide synthesis using recoverable building blocks
ArticleAbstract: (Chemical Equation Presented) The technique of choice for synthesis of small-scale depsipeptides isPalabras claves:Autores:Alberício F., Burger K., Jan Spengler, Ruíz-Rodríguez J.Fuentes:googlescopusA novel protecting/activating strategy for β-hydroxy acids and its use in convergent peptide synthesis
ArticleAbstract: (Chemical Equation Presented) β-Hydroxy acids were reacted with hexafluoroacetone and carbodiimidesPalabras claves:Autores:Alberício F., Burger K., Jan Spengler, Royo M., Ruíz-Rodríguez J., Winter M., Yraola F.Fuentes:googlescopusAmide-to-ester substitution allows fine-tuning of the cyclopeptide conformational ensemble
ArticleAbstract: (Figure Presented) Without affecting the overall 3D structure, amide-to-ester backbone substitutionPalabras claves:Bioorganic chemistry, Conformation analysis, Depsipeptides, Molecular dynamicsNMR spectroscopyAutores:Adan J., Alberício F., Cupido T., Jan Spengler, Mitjans F., Piulats J., Ruíz-Rodríguez J.Fuentes:scopusHomologation of α-hydroxy acids to α-unsubstituted β-hydroxy carboxamides via Arndt-Eistert reaction
ArticleAbstract: Here we studied the homologation of leucic and phenyl lactic acid via Wolff-rearrangement of their dPalabras claves:Microwave shock-heating, α,β-Unsaturated carboxylic acids, α-Hydroxy diazoketones, β-Hydroxy carboxylic acidsAutores:Alberício F., Burger K., Jan Spengler, Ruíz-Rodríguez J.Fuentes:googlescopusSiamese depsipeptides: Constrained bicyclic architectures
ArticleAbstract: The first members of a new class of depsipeptides with tartaric acid as the core unit, called SiamesPalabras claves:biological activity, Bioorganic chemistry, Depsipeptides, Structure-activity relationships, Tartaric acidAutores:Alberício F., Jan Spengler, Ruíz-Rodríguez J.Fuentes:googlescopusTotal regioselective control of tartaric acid
ArticleAbstract: An efficient strategy to synthesize tartaric acid building blocks for totally regioselective transfoPalabras claves:Autores:Alberício F., Burger K., Fernandez-Llamazares A.I., Jan Spengler, Ruíz-Rodríguez J.Fuentes:googlescopus